Non stirred autoclave is mainly used in chemical and material research without mixing experiments. It can be equipped with pressure gauge, intake valve, vent valve, probe pipe, thermocouple and process inlet.
Structure and composition of non agitator high pressure reactor:
1, flexible selection and customization:
all reaction kettle can be customized by customers. High pressure reactor customization range: laboratory reactor, micro reactor, small reaction kettle, and so on.
2, The new fastening structure
Start fastening flange autoclave structure of each test before the preparation period, to the reaction kettle all completely unscrew the bolts, add a good reaction material again and tighten the screw on the back one by one. The opening and sealing process of a single screw needs to be rotated more than ten cycles. There are many bolts in each reactor. The test process is time-consuming and laborious.
The new type autoclave adopts fast opening fastening structure. Compared with the traditional institutions, when each test needs to open the kettle, it can simply pull the screw loose 1 circles or so, so that it can easily take the loop from the side and quickly open the reactor. The tightening process is equally simple and labor-saving. And each ring bolt pressure on the bottom of the cushion ring, the cushion ring press the kettle head, so that the strength of the bolt can be evenly distributed to the cauldron head. In order to ensure uniform force, the traditional flange structure has strict requirements for tightening force and diagonal tightening order, and requires higher operation skills for operators. If a little attention is not paid, it will cause the reaction kettle to leak and retighten the seal.
3, small space double line seal structure:
Polytetrafluoroethylene (PTFE), as an excellent corrosion resistant material, is widely used in the sealing link of the instrument, but it will produce cold flow deformation at 250 degrees.
In order to overcome this contradiction, a new high pressure reactor with precision machining of small space double sealing technology, the kettle head and the kettle body sealing gap is controlled in a very small range, the deformation of PTFE at high temperature, but the gap is too small to engage PTFE cold deformation flow to the external sealing groove, only expansion deformation in the groove, thus to further enhance the sealing of the reactor, and the reactor head and body sealing surface processing V type sealing groove, increase the sealing area. The better the sealing performance is, the higher the temperature is, the higher the temperature is, the better the sealing performance is.
4, The non dead space exploration tube
The laboratory level reaction samples are generally small, and some of the samples are expensive. Therefore, the experimental equipment has obvious influence on the accuracy of the experimental results and the influence of the funds. For example, the hanging wall when adding liquid material is a more prominent problem. The new type of non agitator reactor is through the bottom pipe directly into the cauldron, and there is no dead space in the middle of the transfer head. If the intake is turned into a ball valve, the material can be injected directly into the kettle through a syringe in the middle of the reaction. It is suitable for adding trace amounts of reactants.
5, Strict selection of materials:
The material is very important for the durability and safety of the synthetic kettle. Our company takes the concept of safety and durability. All the main parts of the non stirring kettle are made of high quality stainless steel. The import brand is used to mark the valve pipe fittings and so on, which increases the reliability of the use.
The non stirred high-pressure reactor can be selected with the pressure relief valve, and the maximum use pressure can be set by itself. Ensure the safe use of the reaction kettle.